Microstructure characterization of austenitic Fe–25Mn–22Cr–2Si–0.7N alloy processed by twin roll strip casting

Abstract

Near net shape casting of austenitic stainless steel containing high Mn and N was explored by using a twin roll strip caster. Microstructural observation and analysis of the as-cast strip by XRD, SEM, and TEM demonstrated that the formation of δ-ferrite and carbides had been prohibited due to the high solidification cooling rate of more than 14,000 K/s during strip casting. Tensile tests indicated that the as-cast strip possessed reasonably good mechanical properties, with a yield strength of 500 MPa and elongation of about 15%. The elastic modulus of the as-cast strip was higher than that of solution treated steel by about one order of magnitude. From the TEM observations, it was found that the as-cast strip contained more dislocations and numerous interstitial elements (N and C) dissolved in grains than the solution treated material, in which dislocations were scarcely observed and precipitates were formed along grain boundaries. Fracture morphology indicates that the as-cast strip has undergone ductile rupture during tensile testing. Deformation twins were observed in the deformed region of the sample by the in-situ tensile test under SEM and TEM observations. The formation of deformation twins were believed to be responsible for high plasticity of the as-cast strip.