Abstract

Thispaperaimstoenhance the microstructure, mechanical properties, and tribological properties of Ni3Al matrix composite films (NMCs) and provide efficient and convenient methods for preparing Ni3Al matrix micro-laminate films. Ni3Al/Cr3C2-Ti3SiC2-MoS2 (NMCs-1) single-layer film, as well as Ni3Al/Cr3C2-Ti3SiC2-MoS2 (NMCs-2) and Ni3Al-Cr3C2-MoS2/Ni3Al-Ti3SiC2-MoS2 (NMCs-3) micro-laminated films with different layer thickness ratios were deposited on the surface of GH3044 superalloy using electrohydrodynamic atomization (EHDA). X-ray diffraction, scanning and transmission electron microcopies, and X-ray photoelectron spectroscopy were conducted to analyze and characterize the properties of these films. Results indicated that the NMCs-3 micro-laminated films exhibited denser microstructure, stronger (002) preferred orientation, and higher adhesion to the substrate, compared to the NMCs-1 single-layer film and NMCs-2 micro-laminated films. Additionally, NMCs-3 displayed superior-excellent tribological properties, the wear rate wasreducedby an orderofmagnitude than the NMCs-1 and NMCs-2 films, and the frictioncoefficient fell by 40% comparedwith the film in the previouswork. This was mainly attributed to the inhibition of crack propagation and reduction in film damage through the laminated structuredesign of the NMC-3 films.

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