Abstract
The in-situ Fe based nanocomposite containing Al2O3 particle is synthesized by reactive milling of Fe2O3-Al-Fe powder mixture in toluene medium followed by consolidation of powders using Spark Plasma Sintering process. Transmission electron microscopy investigation of consolidated Fe-Al2O3 nanocomposites has shown heterogenous grain structure of Fe consisting of nano, submicron and micron size grains together with nanometer Al2O3 particles. The hardness of Fe-Al2O3 nanocomposites consolidated at 800°C is 795 MPa.
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