Abstract
Carbon fiber reinforced carbon matrix (C/C) composites are often used for structural and frictional applications at a wide range of temperatures due to their excellent mechanical and thermal properties. Tailoring of mechanical properties through optimization of microstructure is critical for achieving maximum composite performance. This article addresses the evolution of the fiber and matrix microstructure and related nano-mechanical properties in two different C/C composites after being subjected to heat treatment at temperatures between 1800 and 2400 °C. Microstructure and corresponding nano-mechanical properties of C/C composites were studied using Polarized Light Microscopy (PLM), High-Resolution Transmission Electron Microscopy (HRTEM) and nanoindentation techniques. Increased heat treatment temperature (HTT) led to formation of a better-organized microstructure of fiber and matrix and also to formation of thermal cracks. The elastic modulus of rough laminar CVI pyrocarbon decreased from 18 to 12 GPa with increased HTT. In contrast, the isotropic CVI pyrocarbon and charred resin matrix displayed only a slight change of elastic modulus. The elastic modulus of PAN fiber increased from 18 to 34 GPa, indicating the development of a better-organized microstructure in the fiber-axial direction.
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