Microstructure and Deformation Behaviour of Austenitic Low-Density Steels: The Defining Role of B2 Intermetallic Phase

Abstract

The feasibility of significant weight reduction in conjunction with the superior strength-ductility combination makes Fe-Mn-Al-C-based steels the candidate material for automotive and structural applications. The alloy chemistry and processing conditions influence the microstructure in low-density steels (LDS); however, their role in deformation behaviour is not fully understood. In the present study, three different austenitic LDS grades viz. Fe-28Mn-9Al-0.9C, Fe-28Mn-9Al-5Ni-0.9C and Fe-15Mn-9Al-5Ni-0.9C alloys in hot-rolled conditions were used for evaluating the role of secondary phases, especially B2 ordered Fe(Ni)Al phase on deformation characteristics. Ni-free LDS microstructure consisted of the γ-matrix with fine κ-carbides, whereas Ni containing low Mn alloy possessed coarser κ-carbides along with B2 in both bamboo-like stringer and polygonal particle morphology in the γ-matrix. The B2 containing alloy exhibited higher strength with reduced tensile ductility than the B2-free alloy. Hardness of the γ-matrix and B2 phase were similar with B2 grains exhibiting distinct pop-in events in the nanoindentation curves indicating incipient plasticity. The γ-matrix and B2 co-deform near yield, and a favourable orientation relationship (OR) between the γ-matrix and B2 facilitated easy slip transfer, while the non-favourable OR controlled ductility by strain accumulation and B2-cracking. The differences in the strain hardening behaviour of B2-free and B2 containing alloys were elucidated based on the changes in dislocation substructure evolution examined by an automated crystal orientation mapping in electron microscopy.