Abstract

Tube high-pressure shearing (t-HPS) processing was performed on a eutectic Bi–Sn (57/43) alloy for 0.25, 1, 5 and 20 turns. The selected samples were stored at room temperature for up to 56 days to examine the strain weakening and self-annealing behavior of the alloy. The results showed that t-HPS processing gradually refined the microstructure and led to decreasing of microhardness, but microhardness increased slowly during the subsequent storage at room temperature. Shear localization of the eutectic structure during t-HPS processing was observed as large amounts of narrow dense lamellar zones were visible in the deformed microstructures. The Bi–Sn (57/43) alloy processed by t-HPS exhibited significantly enhanced superplastic properties with elongations up to >1800% in a sample after t-HPS processing for 20 turns. This high elongation is attributed to the breaking of the lamellar structure and the very small grain size.

Highlights

  • Considerable interest has developed over the last two decades to producing and measuring the mechanical properties of materials with exceptionally small grain sizes.Ultrafine-grained (UFG) metals are defined as metals where the average grain size is less than ~1 μm [1] and these small grains divide into the two categories of submicrometer grains with sizes of 100–1000 nm and nanometer grains where the average size is

  • As discussed in a comprehensive review [3], the two main techniques of severe plastic deformation (SPD) processing are equal channel angular pressing (ECAP), where a rod or a bar is pressed through a die constrained within a channel bent through a sharp angle [4], and high-pressure torsion (HPT), where the sample is generally in the form of a thin disk subjected to high pressure and concurrent torsional straining [5]

  • Both ECAP and HPT are effective for processing to produce metals with very small grains, but the procedures are different because ECAP is a discontinuous and laborintensive process in which the sample is removed and reinserted into the die between each pass whereas HPT is a continuous process where the sample is torsionally strained up to the required maximum numbers of rotations

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Summary

Introduction

Considerable interest has developed over the last two decades to producing and measuring the mechanical properties of materials with exceptionally small grain sizes.Ultrafine-grained (UFG) metals are defined as metals where the average grain size is less than ~1 μm [1] and these small grains divide into the two categories of submicrometer grains with sizes of 100–1000 nm and nanometer grains where the average size is

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