Abstract
A series of palladium(II) complexes containing bis[(4-isonicotinoyloxy)phenyl]sulfide (L), [PdII(L)(tmen)]2X4 (tmen = N,N,N',N'-tetramethylethane-1,2-diamine; X=NO3 and ClO4) were prepared and characterized. Reaction of [Pd(tmen)](NO3)2 with L in a mixture of water and acetone affords microspheres whereas reaction of [Pd(tmen)](ClO4)2 with L produces microbelts. The solubility of the products is a significant factor for the formation of morphology. The spherical sizes can be controlled by the evaporation rate of solvents. An array of ≈300 nm and ≈4 μm bimodal spheres was carried out via sonication.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
