Abstract
The electrochemical deposition of magnesium from [Mg2(μ-Cl)3·6(OC4H8)]+ has been monitored in situ with X-ray absorption spectroscopy. The viability of the cell design was confirmed by a reversible shift in the X-ray absorption near-edge spectroscopy (XANES) of the Mg K-edge. In situ electrochemical XANES revealed the presence of an interfacial Mg intermediate below the equilibrium Mg/Mg2+ potential. A new method has been established to directly observe the complex electrochemical reduction process from Mg electrolytes.
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