Abstract

There are three independent mol­ecules in the asymmetric unit of the title compound, C9H11NO3, which are connected by O—H⋯O hydrogen bonds, forming an R 3 3(15) ring. The dihedral angles between the planes of the benzene and amide groups are 75.16 (3), 71.47 (3) and 70.56 (3)°. The hy­droxy O atom lies 0.912 (3), 1.172 (2) and 1.339 (2) Å from the mean plane of the corresponding benzene ring in the three mol­ecules.

Highlights

  • There are three independent molecules in the asymmetric unit of the title compound, C9H11NO3, which are connected by O—

  • We are grateful for the help of Professor Jian-Ming Gu of Supplementary data and figures for this paper are available from the

  • There are three independent molecules in the asymmetric unit, which are connected by intermolecular O—H···O hydrogen bonds to construct a large ring involving 15 atoms with graph set notation R33(15) (Fig. 2)

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Summary

Data collection

Catalytic Hydrogenation Research Center, Zhejiang University of Technology, Hangzhou 310014, People’s Republic of China. R factor = 0.063; wR factor = 0.161; data-to-parameter ratio = 15.6. There are three independent molecules in the asymmetric unit of the title compound, C9H11NO3, which are connected by O—. H O hydrogen bonds, forming an R33(15) ring. The dihedral angles between the planes of the benzene and amide groups are 75.16 (3), 71.47 (3) and 70.56 (3). The hydroxy O atom lies 0.912 (3), 1.172 (2) and 1.339 (2) Å from the mean plane of the corresponding benzene ring in the three molecules

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