Abstract
There are three independent molecules in the asymmetric unit of the title compound, C9H11NO3, which are connected by O—H⋯O hydrogen bonds, forming an R 3 3(15) ring. The dihedral angles between the planes of the benzene and amide groups are 75.16 (3), 71.47 (3) and 70.56 (3)°. The hydroxy O atom lies 0.912 (3), 1.172 (2) and 1.339 (2) Å from the mean plane of the corresponding benzene ring in the three molecules.
Highlights
There are three independent molecules in the asymmetric unit of the title compound, C9H11NO3, which are connected by O—
We are grateful for the help of Professor Jian-Ming Gu of Supplementary data and figures for this paper are available from the
There are three independent molecules in the asymmetric unit, which are connected by intermolecular O—H···O hydrogen bonds to construct a large ring involving 15 atoms with graph set notation R33(15) (Fig. 2)
Summary
Catalytic Hydrogenation Research Center, Zhejiang University of Technology, Hangzhou 310014, People’s Republic of China. R factor = 0.063; wR factor = 0.161; data-to-parameter ratio = 15.6. There are three independent molecules in the asymmetric unit of the title compound, C9H11NO3, which are connected by O—. H O hydrogen bonds, forming an R33(15) ring. The dihedral angles between the planes of the benzene and amide groups are 75.16 (3), 71.47 (3) and 70.56 (3). The hydroxy O atom lies 0.912 (3), 1.172 (2) and 1.339 (2) Å from the mean plane of the corresponding benzene ring in the three molecules
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