Abstract
AbstractIn this paper we describe the synthesis and intercomparison of several new methanofullerenes, each bearing a macrocyclic crown ether containing a malonate moiety directly attached to the C60‐fullerene core. Their complexing abilities with primary alkylammonium ions were investigated by NMR and mass spectrometry, and also by transport experiments through a liquid membrane. We also report on their electrochemical behaviour, together with EPR analysis of their supramolecular complexes with alkyl ammonium molecules labelled with a stable nitroxide radical. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)
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