Abstract

AbstractA mild and effective method for the synthesis of 2‐C‐branched disaccharides, glycoconjugates, and nucleoside analogues is described. 1,2‐(acetylcyclopropane)‐annulated D‐lyxofuranose underwent ring opening catalysed by CH3SO3H to act as an efficient glycosyl donor and give the glycosylation products in good yields and with high diastereoselectivities.

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