Abstract
A combination of pillar[5]-bis-trithiacrown (L) and mercury(ii) halides afforded a monomer complex (Cl--form), a 1-D coordination polymer (Br--form) and a supramolecular ion-triplet complex [(I·Hg·I)@L] (I--form). In the ion-triplet complex, the host encapsulates the (I--Hg2+-I-) entity via Hg2+π and C-HI- interactions, reflecting geometrical complementarity.
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