Abstract
AbstractM9‐ and M12‐metal clusters appear as face‐sharing double‐clusters in (Pb9Br19)2(Pb1.5Br2)2(melem)3 (6) and as triple‐clusters in (Pb12Br25)4(Pb1.67Br2)3(melem)4 (7). All compounds are characterized by single‐crystal and powder X‐ray diffraction, and further validated by infrared (IR) spectroscopy and 207Pb and 79/81Br NMR studies on (5). Photoluminescence studies on compound (6) reveal emission at 430 nm while the emission of (5) is completely quenched.
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