Abstract
A phase transformation of σ-CrFe to the bcc solid solution during high-energy ball milling was monitored by X-ray diffraction, AC susceptibility and high-field magnetization measurements. The saturation magnetization shows a maximum as a function of milling time. The increase is ascribed to the phase transformation, the decrease during further milling to the generation of nanocrystalline material. The phase transformation from the σ-phase to the solid solution is discussed in terms of Miedema's semi-empirical model.
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