Mechanical properties and bond strength of dual-cure resin composites to root canal dentin

Abstract

Objectives To evaluate the regional mechanical properties of dual-cure resin composites and their regional bond strengths to root canal dentin. Methods One of the following dual-cure resin composites was placed in artificial post spaces: Unifil Core (UC), Clearfil DC Core (DC), Build-It FR (BI), Clearfil DC Core-automix (DCA), and photo-cured for 60 s. After 24 h storage, each specimen was serially sliced to harvest eight hour-glass shaped specimens for measurement of regional ultimate tensile strength (UTS), and the remaining eight semi-circular slabs were polished for the measurement of Knoop Hardness Number (KHN). For the microtensile bond strength (μTBS) test, post cavities were prepared in human premolar roots, and the cavity surfaces treated with Clearfil SE Bond and photo-cured for 10 s. The post spaces were then filled with one of the above resin composites and photo-cured for 60 s. After 24 h storage, each specimen was serially sliced into 8, 0.6 × 0.6 mm-thick beams for the μTBS test. The data were divided into coronal and apical regions and analyzed using ANOVA and post hoc test ( α = 0.05). Results UTS and KHN were affected by the type of dual-cure resin composite and region ( p < 0.0001). There was no relationship between UTS and KHN for each material. The auto-mix type of resin composite possessed superior UTS to that of the hand-mix type. μTBS among the four composite materials were not significantly different at both apical and coronal regions ( p > 0.05). Regional differences in bond strengths were found for all materials ( p < 0.05). Significance The UTS and KHN of the dual-cure resin composites varied among each material, however, differences in the mechanical properties of the resin core materials did not affect their adhesion to root canal dentin.