Mechanical experiment evaluation of the microvascular self-healing capability of bitumen using hollow fibers containing oily rejuvenator

Abstract

Smart microvascular self-healing bituminous composites are considered a promising approach to prolong pavement service life. The objective of this work was to investigate the microvascular self-healing capability of bituminous material by using hollow fibers with oily rejuvenator through a direct-tension mechanical experiment. The hollow fibers with oily rejuvenator were prepared using a wet-spinning approach by applying polyvinylidene fluoride material. The fixed-length hollow fibers with sealed ends were mixed in bitumen to form composite samples. Through a repetitive tensile method, the tension strength data were used to calculate the self-healing efficiency autonomously by considering crack closure and healing at various healing temperatures and times. The scanning-electron-microscope morphology showed that the polyvinylidene fluoride hollow fibers had a tight interfacial structure with bituminous material without debonding. X-ray computed tomography results indicated that the fibers were distributed homogeneously in bitumen. The fiber content and fiber orientation affected the self-healing capability of bituminous samples at 0 °C. To simplify the influence of the above two factors of the fibers, only one fiber was placed in bitumen samples parallel to the tension direction. With an increase in temperature from 0 to 30 °C, the self-healing capability of the bitumen samples increased dramatically. This phenomenon is attributed to the accelerated penetration speed of rejuvenator in the bitumen. An increase in time increased the self-healing capability of the bitumen samples. The rejuvenator may have sufficient time to leak from the hollow fibers and penetrate the bitumen. The results provide a guide to the microstructural design of the vascular fibers and the application of hollow fibers in self-healing asphalt pavement.