Abstract
Mass spectra of Fe 3(CO) 9X 2 (X S, Se, Te) and Fe 2(CO) 6X′ 2 (X′ S, Se) are recorded and their fragmentation pattern given. The thermal decarbonylation has been studied using DTA/TG methods in the temperature range 25–600°C. The results are compared with those obtained from mass-spectroscopic studies. X-ray and magnetic measurements have been carried out on the residues obtained in the decarbonylation process.
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