Abstract
Nanocrystalline iron–nickel alloys are electrodeposited by direct and pulse current densities with the grain sizes between 8–16 nm. XRD patterns showed a variety of structure in alloys from fcc, bcc and mixed (fcc+bcc) by variation of Fe content of alloy. The fcc structure was observed for lower Fe content, dual phase structure for Fe content between 60–70% and bcc structure for higher Fe content. By applying pulse current, an increase in Fe content of alloys was observed. Magnetic property measurements showed a high saturation magnetization for the alloys increased with increase in Fe content and a low coercivity decreased with decrease in grain size for alloys with iron content below 60%.
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