Abstract
A number of related compounds containing rhodium–carbon bonds have been examined by 1H and 19F single-resonance and 1H-{19F}, 1H-{31P}, 1H-{103Rh}, 19F-{31P}, and 19F-{103Rh} double-resonance n.m.r. spectroscopy. Chemical shifts and signs and magnitudes of coupling constants involving these nuclei are presented and discussed.
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