Abstract
A highly active, genuinely heterogeneous catalyst for liquid-phase Diels–Alder reactions of enones results from the silanol centred modification of an incompletely condensed silasesquioxane with trimethylaluminium, the resulting catalytic material being a gel that contains aluminium(III) siloxy functions (Al–O–Si) which are incorporated in a well defined, three-dimensional SiO framework.
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