Abstract
Single crystal nanoflakes and nanorods of Ni(OH) 2, Co(OH) 2 and Fe 3O 4 were prepared by a controlled hydrothermal conversion route from MC 2O 4·2H 2O in the NaOH solution. The structure and morphology of the final products and their oxalate precursors were characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM). The formation mechanism of conversion was suggested in this paper, accompanied the morphology control hypothesis.
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