Abstract
Reaction of NiCl2 · 6H2O and P(CH2OH)3 (THP) with H2S and (H7O3)2[Mo6Cl14] · 3H2O in ethanol produces new trinuclear nickel sulphide complex [Ni3(μ3-S)2{(HOCH2)2PCH2OP(CH2OH)2}3][Mo6Cl14] · 0.8H2O (I) with new bidentate phosphine-phosphinite ligand resulted from THP condensation. It was characterized by X-ray structure analysis.
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