Abstract

This analytical study of Globucid (sulphanilaminoethylthiodiazole) comprises : l. The determination of physical constants, melting-point and solubilities, of the compound. 2. The identification of the different functional groups, arylamine, substituted benzene, sulphonamide and tests for aminoethylthiodiazole by colour and precipitation reactions, as well as a number of precipitation and microchemical reactions of Globucid itself. 3. A quantitative section : determination of total nitrogen and thiodiazole nitrogen by difference, determination of amino nitrogen, acidimetric and argentometric determination of the sulphonamide groups, determination of total sulphur and thiodiazole sulphur and finally bromometric assay of Globucid.

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