Abstract

Scanning electron microscopy reveals that the structure of the Ag electrode is notably altered by laser illumination during electrochemical oxidation and reduction in 1 M KX (X = 1, Br, Cl, and F) electrolytes. Laser illumination also influences the voltammogram in 1 M Kl, the intensities of the SERS of adsorbed H 2O and pyridine, and the intensities of selected points in the featureless background of the SERS spectra.

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