Laboratory Study of Micro-shear Bond Strength of Two Resin Cements to Leucite Ceramics using Different Ceramic Primers

Abstract

To evaluate the effect of Monobond Etch & Prime on the micro-shear bond strength (MSBS) of resin cements to leucite surface and to compare the MSBS of two different resin cements to conditioned leucite surfaces with different primer systems. Twenty-one leucite ceramic disks (10 mm diameter, 2 mm thickness) were divided into three groups (n = 7). Group I: 9.6% hydrofluoric (HF) acid and Monobond S (Ivoclar Vivadent, Liechtenstein), then conventional resin cement was applied. Group II: Monobond Etch & Prime (Ivoclar Vivadent, Liechtenstein), then conventional resin cement was applied. Group III: 9.6% HF acid and with Monobond N (Ivoclar Vivadent, Liechtenstein), then adhesive resin cement was applied. The assigned resin cement was applied in each disk through five plastic tubes with an inner diameter of 1.6 and 1.9 mm height, and then light cured. Micro-shear bond strength was determined by pulling out the resin cement using universal testing machine (Instron®, USA). One-way analysis of variance (ANOVA) and Student's t-test were used to determine statistical difference (a = 0.05) between each two groups. The results showed that group III had the highest MSBS values (7.32 ± 2.47) followed by group II (6.24 ± 2.16), whereas group I had the lowest MSBS values (5.7 ± 2.7). Nevertheless, there was no statistically significant difference between the results of all the groups. Monobond Etch & Prime has shown comparable results to the most popular combination of HF acid and silane. The combination of HF acid and Monobond N and self-adhesive resin cement has shown the best MSBS results, though not statistically significant. The clinicians can use simplified ceramic primer technique (Monobond Etch & Prime) which has comparable MSBS to the most popular combination of HF acid and silane.