Abstract
The deprotection of amines may be conducted via the cathodic cleavage of the corresponding sulfonamides. However, the selectivity of the reaction depends on parameters such as the tendency of the sulfonamide in the absence of proton donors to be decomposed into imine at the cathodic interface. The problem is discussed as a function of the molecular structure of the starting sulfonamide. Results on simple sulfonomides are applied successfully in the deprotection of polysulfonamides and may allow the synthesis of new polyazaligonds.
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