Abstract
Three different arsonium salts were prepared by a solvent‐free method from Ph3As and the respective 2‐bromoacetophenones. These salts were deprotonated by NaOH to form keto‐stabilized arsenic ylides. The ylids react with [AuCl(tht)] affording gold(I) complexes containing the C‐bound ylide. The compounds were characterized by NMR spectroscopy, IR spectroscopy, and X‐ray diffraction.
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