Abstract
The first example of ivy-like extended structure based on Ni mono-substituted Keggin polyoxomolybdate has been hydrothermally synthesized and characterized. The distorted organic bicapped Keggin POM modified by uncoordinated 4,4΄-bpys serves as an unprecedented synthon for the supramolecular assembly of 3-D frameworks through strong π⋯π stacking interactions. The compound could serve as a potential catalyst in the oxidation of styrene to benzaldehyde.
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