Abstract
The organopalladium(II) complex [Pd(OClO 3)(DMPP){( S-CH 3CH(1-C 10H 6)NMe 2}] (where DMPP = 1-phenyl-3,4-dimethylphosphole) has been isolated. X-ray structural analysis of this reactive complex in the solid state revealed that the perchlorato ligand is bonded to Pd via one of its oxygen atoms and the DMPP is coordinated as a mondentate ligand via phosphorus. In non-coordinating solvents, conductivity measurements confirmed that the PdOClO 3 bond is retained.
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