Abstract
Trifluoromethanesulfonate and tetrafluoroborate salts of the previously in situ-generated synthetic precursor [Tp*W(NCMe)(CO) 3 ] + and a propionitrile analogue, [Tp*W(NCEt)(CO) 3 ](CF 3 SO 3 ), have been isolated and fully characterized. The complex cations exhibit a carbonyl-capped octahedral structure with C s symmetry and undergo slow nitrile ligand exchange.
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