Abstract

This work describes the concentration of iron ore slimes on a pilot scale by using a 500-mm diameter flotation column and a novel collector, which renders the use of a depressant unnecessary. The pilot column was operated in series with the industrial plant Vargem Grande 2 (Iron Quadrangle, Brazil) receiving, as feed, part of the underflow from the desliming thickener. These pilot tests represented only the rougher stage of a flotation circuit. The novel collector used was an amidoamine (average collector dosage of 160 g/t), and the tests were carried out in the absence of starch, at pH 10.5 and with bubbles/microbubbles generated by cavitation tube. It was possible to achieve a concentrate, by reverse flotation, with an average iron content of 53% and an average metallurgical recovery of 91.5% The recovery of the silica in the froth was 53.1% in average for one stage of flotation. The high variability of the slime characteristics rendered difficult the stabilization of the SiO2 recovery; however, the applicability of the amidoamine collector was proven. In an industrial scale circuit, the use of online analyzers for Fe and SiO2 content and the adoption of control logics based on the adjustment of parameters such as reagents dosage and washing water flow rate adjustment should contribute to the optimization of the results obtained in the pilot scale tests. Further studies adding a cleaner concentration stage should be performed.

Highlights

  • Achaye [3] showed that froth stability decreases with increasing particle size and fine particles had the greatest influence on froth stability

  • This paper presents the results of the continuous pilot campaign of reverse cationic flotation of the iron ore slimes combining column flotation and a new collector reagent avoiding the use of a depressant, showing the fluctuation of some slimes characteristics in an industrial plant and discussing the effect of some operational parameters on the iron ore slime flotation performances

  • Results reported by Matiolo et al [27] adopted a singular sample to carry out pilot slime flotation column tests using the amidoamine Flotinor 5530 as a collector without starch, where it was possible to achieve iron grades of approximately 62% in the concentrate and 8% in the tailings; there are no concentration plants by flotation for itabirite iron ore consisting of one single stage

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Summary

Introduction

The harmful effect of slime on quartz reverse flotation has been known since the beginning of iron ore flotation operations. The removal of slimes using hydrocyclones was introduced by United States Bureau of Mines (USBM) [1]. The high consumption of reagents and the difficulty to remove ultrafine quartz and the high amount of deleterious minerals, such as kaolinite, are the main issues due to the presence of slimes in the flotation [2]. The high stability of the froth is an important characteristic regarding slimes presence in flotation systems. Some authors [4,5] investigated the relationship between froth stability, size distribution, and air recovery, demonstrating there is an ideal air rate for each particle size distribution

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