Abstract
AbstractThe iron‐catalyzed homocoupling reaction of aryl Grignard reagent was completed very quickly when the reaction was carried out in a phosphonium salt ionic liquid solvent system at 0°C for 5 min. Using a similar reaction system, the first example of the iron‐catalyzed homocoupling reaction of alkynyl Grignard reagents has also been accomplished using the ionic liquid technology. © 2011 Wiley Periodicals, Inc. Heteroatom Chem 22:397–404, 2011; View this article online at wileyonlinelibrary.com. DOI 10.1002/hc.20696
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