Abstract
AbstractA tandem Ir(III)‐catalyzed and Ag2O‐promoted cross‐dehydrogenative coupling (CDC)/ intramolecular cyclization of ketene dithioacetals with benzothiophene derivatives was developed, affording a series of sulfur‐containing cyclization compounds. Mechanistic investigation demonstrated a radical process may be involving intramolecular cyclization. This tandem reaction described herein could be carried out with a broad range of substrates and wide functional group tolerance.magnified image
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