Abstract
Alkyl and aryl thiols have been determined in the presence of carboxylic acids and phenols by means of acid-base catalytic thermometric titrimetry. Two titrations are carried out, with acrylonitrile and acetone as the end-point indicators. With the former indicator, thiol groups are not determined, so that the difference between the titration values obtained by using the two methods of end-point indication is a measure of the thiol content.
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