Abstract
A molecular salt with a bulky cation and anion, (H2bipip)(H)2[Fe(CN)6] (1) (H2bipip2+: 4,4′-bipiperidine-1,1′-diium), has been prepared. The salt comprises protons (H+) as counter cations. Single-crystal X-ray structure analysis revealed that the proton is trapped between two cyanido ligands of [Fe(CN)6]4− anions, forming a very short N⋯H+⋯N hydrogen bond.
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