Abstract
The thallium form of the narrow-pore zeolite natrolite has been studied with the aid of NMR spectroscopy, scanning calorimetry, and x-ray powder diffraction analysis. A phase transition accompanied by an abrupt change in the mobility of the TI + ions and H=O molecules has been discovered at T = 252 K. The transition may be regarded as "melting" of the aqueous and cation sublattices in the channels of the zeolite skeleton.
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