Abstract

Time-resolved characterization methods provide fundamental insights into electrode processes by capturing events that occur at short time scales. We recently developed the electrochemical real-time mass spectrometry (EC-RTMS) to determine gaseous and liquid products of electrochemical reactions shortly after their formation, with resolution in the order of few seconds. After describing its basic components, I will present some representative examples of using EC-RTMS to monitor the products of CO2 reduction under dynamic conditions, on various copper electrodes.

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