Abstract
The mechanism of the electrochemical reduction of dithizone to the corresponding hydrazo compound, diphenylthiocarbazide, has been examined in detail by polarographic and voltammetric techniques over a wide pH range. The reaction is reversible and dithizone can be determined polarographically in the range 10 -3–10 -5 M. This polarographic behaviour suggests new applications of dithizone as an electroanalytical reagent.
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