Abstract

Thermal energy storage is one of the promising technologies in the modern era for balancing the peak power demand without emitting much emission. Molten-salt technology plays a dominant role among the varieties of thermal energy storage systems. The difficulty in storing the molten-salt technology requires a storage material with high temperature, corrosion, and oxidation resistance properties. The nickel-based superalloys such as Inconel 625 and Incoloy 800H possess the desired properties to be used as a storage material for the molten salts. In this present work, the Incoloy 800H and Inconel 625 superalloy specimens were taken up for investigation. The specimens were coated with yttria-stabilized zirconia as a thermal barrier coating using a plasma spray process. The sodium chloride and potassium chloride molten salts with a weight fraction of 7 : 3 have been taken with both uncoated and YSZ-coated specimens, and specimens were heated up to 1000°C approximately. The specimens were heated for different hours such as 8, 12, and 16 hours, respectively. The increase in heating time also results in the increase in the tensile property of the specimens. The mechanical testing, such as tensile test and hardness test, was performed to comprehend the mechanical properties. Scanning electron microscope images and X-ray diffraction analysis were made to study the microstructural properties and the corrosion resistance property. From the test results, YSZ-coated specimens possess high corrosion resistance and high mechanical strength compared to the uncoated specimens.

Highlights

  • Superalloys are an alloy with a high-melting point capability

  • After the heating process of specimens with different hours, the specimens were tested with the tensile test and hardness test

  • The tensile test conducted on 8-hour-heated specimens result in yield strength of 243 MPa, ultimate tensile strength of 551 MPa, and % of elongation of 38.00 in 25 mm gauge length

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Summary

Introduction

Superalloys are an alloy with a high-melting point capability. It includes the outstanding mechanical strength, thermal deformation resistance, good surface stability, and corrosion or oxidation resistance. Super alloys are mostly formed as one single crystal, which increases creep resistance while the grain boundaries may provide strength at low temperatures. Inconel 625 is used for its high strength, excellent fabricability (including joining), and outstanding corrosion resistance. Incoloy 800H possesses chemical properties for high-temperature strength and resistance to oxidation, carburization, and other high-temperature corrosion. Incoloy 800H has high nickel and chromium content, and this helps in resisting oxidation. A protective surface oxide is formed due to the presence of chromium, and nickel will provide the additional protection during continuous exposure

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