Abstract
The analytical potential of a non-dispersive atomic fluorescence spectrometer with a tantalum coil atomizer for gas monitoring are investigated. The analytical procedure for the determination of iron in argon, introduced as iron pentacarbonyl, is suggested as a first step of reactive gas monitoring. Parameters optimized include the atomization temperature and duration time and the atom residence time in the atomizer. These parameters are optimized by varying the charge voltage and condenser capacity. The detection limit achieved for iron is 4 ng l–1 of gas. The relative standard deviation sr= 0.03.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.