Abstract
[FeCl{η2-Ph2PCHC(R)S}(PMe3)(CO)(L)] complexes, prepared by ligand substitution, react with phenylacetylene in the presence of AgBF4 or NaPF6 and lead to carbon–sulphur bond formation between the β-phosphino–thioenolate ligand and the phenylvinylidene–iron intermediate, as shown by X-ray diffraction analysis.
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