Abstract
Single-crystal X-ray diffraction is used to determine the structure of a new compound based on an octahedral cyanide anionic cluster complex of rhenium and a trimethyltin(IV) cation: {(SnMe3)3[Re6Se8(CN)6]} (1). The crystallographic characteristics: space group C2/c, a = 13.9898(14) A, b =15.334(2) A, c = 20.761(2) A, β = 97.75(0)°, V = 4412.91(90) A3, Z = 4, d x = 3.607 g/cm3, and R = 0.0526. The compound has a framework structure; two porous frameworks with pcu topology interpenetrate each other.
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