Abstract
The internal mobility of fluorine ions and the electrophysical properties of TlSb2F7 were studied by the 19F NMR method and impedance spectroscopy. Modes of ionic motions in the fluoride subsystem were determined in the temperature range 213–430 K. A structural phase transition is found to occur at 400 K, resulting in the β‐TlSb2F7 modification characterized by high ionic (superionic) conductivity in the temperature range of 400–430 K σ∼ 2.5·10-3 S/cm at 430 K).
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