Abstract

Multi-keV X-ray microscopy has been particularly successful in bridging the resolution gap between optical and electron microscopy. However, resolutions below 20 nm are still considered challenging, as high throughput direct imaging methods are limited by the availability of suitable optical elements. In order to bridge this gap, we present a new type of Fresnel zone plate lenses aimed at the sub-20 and the sub-10 nm resolution range. By extending the concept of double-sided zone plate stacking, we demonstrate the doubling of the effective line density and thus the resolution and provide large aperture, singlechip optical devices with 15 and 7 nm smallest zone widths. The detailed characterization of these lenses shows excellent optical properties with focal spots down to 7.8 nm. Beyond wave front characterization, the zone plates also excel in typical imaging scenarios, verifying their resolution close to their diffraction limited optical performance.

Highlights

  • A longstanding dream of many scientists is a microscope offering the complementary capabilities of optical and electron microscopy while bridging the resolution gap between these two methods

  • As an alternative to mechanical stacking, we have shown that the every-day use can be greatly simplified by fabricating the two partial zone plates on both sides of the same support membrane[30,31]

  • We report on the fabrication and characterization of two sets of double-sided, line-doubled Fresnel zone plates with 100 microns aperture size

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Summary

Introduction

A longstanding dream of many scientists is a microscope offering the complementary capabilities of optical and electron microscopy while bridging the resolution gap between these two methods. Diffractive X-ray optics, such as Fresnel zone plates[12], are widely used as objective lenses for both scanning probe and full-field X-ray microscopy These diffractive lenses can be described as circular gratings with decreasing periodicity towards their outer edge. The combined zone plate exhibits half the periodicity and double the resolution as the fabricated individual partial zone plates This approach is analogous to frequency doubling via interlacing in cathode-ray tube TVs and monitors, whereas the scanning electron beam draws only every even or odd line to double the refresh rate. Both partial zone plates can be fabricated using the zone doubling technique[13,29]. This method avoids the patterning of very narrow resist structures as required for conventional zone-doubling

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