Abstract

The alkoxy radicals derived from cyclic hemiacetals are generated through visible‐light‐induced electron transfer with NaI and Ph3P as the catalyst. Subsequent β‐scission generates carbon‐centered radicals, which are trapped by cinnamic acids, aryl alkenes, vinylboronic acid and silyl enol ether to deliver the corresponding C—C bond forming products. More details are discussed in the article by Wang et al. on page 259–264.image

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