Abstract
The reaction between [Pd {C 6H 4CH 2 NCH(2,6-C 6H 3Cl 2)}Br] 2 and PhCCPh gives the bis-insertion compound [Pd {(PhCCPh) 2C 6H 4CH 2 NCH(2,6-C 6H 3Cl 2} Br] in good yield. This compound crystallizes in the monoclinic space group P2 1/ a, with a 18.757(3), b 15.678(3), c, 12.150(2) Å β 92.83(2)° and Z = 4; R = 0.063 for 2076 reflections. The palladium atom is coordinated to Br, N, C(18), and the centre of the C(15)–C(16) double bond in a distorted square-planar geometry.
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