Abstract
A simple specular reflectance method is described for obtaining the infra red spectra of species in the electrode/electrolyte solution interphase. The method is shown to be sufficiently sensitive to enable aqueous electrolytes to be used. Results are presented indicating the existence of discrete water structures, resembling small clusters of water molecules, in the inner region of the double layer at platinum and electrodes. Preliminary data are also given for adsorbed hydrogen on a platinum electrode.
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