Influence of surface treatments on the bond strength of metal brackets to CAD/CAM materials and discoloration after various refinishing procedures : Scanning electron microscopy and atomic force microscopy study.

Abstract

This study evaluated the shear bond strength (SBS) of ametal bracket bonded to three different computer-aided design/computer-aided manufacturing (CAD/CAM) restoration materials pretreated with different surface treatments. In addition, the surface topography and color change of the restorations after debonding with two different tungsten carbide burs were examined. A total of 216plates were cut from three different CAD/CAM blocks, each of which was divided into three subgroups with different pretreatment methods: (1)acid etching, (2)sandblasting, and (3)laser irradiation. Incisor metal brackets were bonded. The SBS test was performed, and the failure types were classified. Then, samples were randomly divided into two subgroups according to the adhesive removal procedure to be used: atungsten carbide bur with 12blades or 24blades (n = 12). Color change was calculated based on the ∆E00, and surface morphology was evaluated via SEM and AFM analysis. The SBS data revealed that the type of CAD/CAM material and the applied surface treatment significantly affected bond strength. The highest SBS values were detected for the Grandio Blocs (VOCO GmbH, Cuxhaven, Germany; 14.3 ± 4.4 MPa), and the lowest was observed for Cerasmart (GC Europe, Leuven, Belgium; 12.0 ± 4.0 MPa). The ∆E00 results demonstrated significant differences only as aresult of the applied surface treatment. The ∆E00 value in all groups was above the 1.77 threshold. CAD/CAM material types and surface treatments affected the bond strength, but the interactions of these factors did not. The chosen surface treatment also significantly affected the ∆E00 after the polishing was done.