Influence of sintering pressure on the microstructure and tribological properties of low temperature fast sintered hot-pressed Y-TZP

Abstract

Contrarily to conventional sintering (CS) method where longer cycles and high temperature (1400–1500 °C) are applied to sinter yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramics, this work presents a faster and low temperature (1175 °C) way through hot pressing (HP) to produce full densified zirconia with good mechanical and tribological properties. This work is concerned with the influence of sintering pressure on the microstructure and tribological properties of hot-pressed Y-TZP. For this purpose, four sintering pressures 5, 20, 60 and 100 MPa were tested. The wear tests were carried out by reciprocating ball-on-plate as a simplified test for tooth-to-restorative material contact under 37 °C using artificial saliva to mimic oral conditions. The results demonstrated that density, hardness and tribological properties are strongly influenced by the sintering pressure, namely an improvement with pressure increase was achieved. The highest density, hardness values and wear resistance were achieved for Y-TZP samples produced at P = 100 MPa. Furthermore, it was revealed that a smaller grain size for Z100 samples (full densification condition) was achieved comparatively to conventional-sintered Y-TZP. This work proves that it is possible to produce dense Y-TZP materials under low sintering temperature and faster cycles with reduced grain size without compromise mechanical and tribological properties.