Abstract
Friction stir extrusion (FSE) was used with WE43 Mg to create a rod with a hybrid microstructure. The rod’s electrochemical corrosion response was characterized in Hank’s balanced salt solution at 37 ± 1 °C. The rod showed refined grains near the edge, while coarse grains were observed at the rod center. A larger fraction of precipitates was observed near the edge possibly hindering grain growth. The refined grains and the presence of a larger fraction of precipitates in the edge regions resulted in higher hardness owing to a confluence of precipitate hardening and solid–solution strengthening. Texture analysis of the rod cross-section exhibited a basal texture, perpendicular to the extrusion direction and populating the rod’s outer surface. In compression, the rod showed a near-base material yield strength (225.6 MPa) and a good combination of compressive strength (357.5 MPa) and ductility (~17.7%). The rod’s electrochemical corrosion response was sensitive to variations in the grain size, texture, and precipitate distribution between the rod core and edge regions. Removal of the edge region resulted in the formation of a more stable and protective film with an increase in the immersion period. The results from the study establish the ability of the FSE process to tailor the rod microstructure thereby influencing the mechanical properties and corrosion rate of Mg alloy.
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